Siyanbola, T. O. and Anjaneyulu, B. and Narayan, R. and Olaofe, O. and Akintayo, E. T. and Rao, B. V. S. K. and Prasad, R and Raju, KVSN (2011) Synthesis and Characterization of Polyamide-Urethane/Clay Nanocomposites from Yellow Oleanda (Thevetia Peruviana) Seed Oil. In: 66th Annual Convention of OTAI, November 18-19, 2011, CSIR- Indian Institute of Chemical Technology Hyderabad - 500 007, India.
![[img]](http://eprints.covenantuniversity.edu.ng/style/images/fileicons/application_pdf.png) |
PDF
Download (1MB) |
Abstract
Thevetia peruviana commonly known as yellow oleanda or lucky nut seed oil was harvested in EmureEkiti, southwestern Nigeria. The extraction of the seed oil was carried out using n-hexane in a soxhlet extractor. The seed oil with high contents of 18:1 (48.24%), 16:0 (22.25%), 18:2 (19.76%) fatty acids and having the following physico-chemical parameters (I.V, 75.4; S.V, 192.5; P. V, 1.9; A.V, 2.0; specific gravity, 0.91175; density, 0.90905. The seed oil was used in the preparation of diethanolamide. The diethanolamide was subsequently used in the preparation of polyurethane/clay nanocomposite. The formation of the hybrid polymeric coating was monitored and confirmed using Fourier Transform Infrared Spectroscopy (Ff-IR), Nuclear Magnetic Resonance (IH-NMR and 13C-NMR), Electronspin ionization-mass spectroscopy (ESIMS), X-ray diffraction spectroscopy (XRD). The thermal stability of the product was studied by Thermal gravimetic analyser (TGA), Dynamic and mechanical thermal analyser (DMTA), Differential scanning calorimetry (DSC).
| Item Type: | Conference or Workshop Item (Paper) |
|---|---|
| Subjects: | Q Science > QD Chemistry |
| Divisions: | Faculty of Engineering, Science and Mathematics > School of Chemistry |
| Depositing User: | Mrs Patricia Nwokealisi |
| Date Deposited: | 18 Jan 2017 16:04 |
| Last Modified: | 18 Jan 2017 16:04 |
| URI: | http://eprints.covenantuniversity.edu.ng/id/eprint/7577 |
Actions (login required)
 |
View Item |
